Propanoic acid, 2-bromo-2-methyl-, ethyl ester → ethyl(+/-)-5-dodecyl-alpha,alpha-dimethyl-2H-tetrazole-2-acetate

HRID 264068

反応式

HRID 264068 の反応式
[CH2:1]([C:13]1[NH:17][N:16]=[N:15][N:14]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].C(C1NN=NN=1)CCCCCCCCC.[CH2:33]([O:35][C:36](=[O:41])[C:37](Br)([CH3:39])[CH3:38])[CH3:34].BrC1C=CC=CC=1CC(OCC)=O>>[CH2:1]([C:13]1[N:14]=[N:15][N:16]([C:37]([CH3:39])([CH3:38])[C:36]([O:35][CH2:33][CH3:34])=[O:41])[N:17]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]

参加物

5

反応物 4

HCID 11745Propanoic acid, 2-bromo-2-methyl-, ethyl esterHCID 2780092Ethyl 2-(2-bromophenyl)acetateHCID 178442802HCID 178442802、化合物HCID 178442834HCID 178442834、化合物

生成物 1

HCID 18955384ethyl(+/-)-5-dodecyl-alpha,alpha-dimethyl-2H-tetrazole-2-acetate

実験手順

When in the general procedure of Example 71 an appropriate amount of 5-dodecyl-1H-tetrazole was substituted for 5-decyl-1H-tetrazole and an appropriate amount of ethyl-2-bromoisobutyrate was substituted for ethyl 2-bromophenylacetate, the title compound was obtained.

出典と根拠

ORDレコード
ord-aadaceb2ac214d119453726570a39ee9
出典データセット
uspto-grants-1997_07
特許番号
US05646170

関連ノート

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