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HRID 264351作成日:2026年10月25日

Methyl Gentisate → Methyl 5-(2-cyclohexylethoxy)-2-hydroxybenzoate

https://huagongshe.com/reaction/264351

反応式

関与物質

役割名称HCID仕込み量
反応物Methyl GentisateHCID 75077—
反応物2-Cyclohexylethyl 4-methylbenzenesulfonateHCID 11426070—
生成物Methyl 5-(2-cyclohexylethoxy)-2-hydroxybenzoateHCID 1903672343%

反応手順

Synthesis was carried out in the same manner as in Example 1, except for replacing methyl 2,4-dihydroxybenzoate with methyl 2,5-dihydroxybenzoate and replacing 2-ethylhexyl bromide with 2-cyclohexylethyl p-toluenesulfonate, to obtain methyl 5-(2-cyclohexylethoxy)-2-hydroxybenzoate represented by the following chemical formula (hereinafter referred to as compound 11) as a pale yellow solid in a yield of 43%. The analytical results are shown below. ##STR32##

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05646184
出典データセットuspto-grants-1997_07
ORD IDord-dde65f479bc54da9b6f090eb6743d7ff
出典メモuspto-grants-1997_07