化工社化工社 化学情報印刷レポート · 研究参考用
Methyl Gentisate → Methyl 5-(2-cyclohexylethoxy)-2-hydroxybenzoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl Gentisate | HCID 75077 | — |
| 反応物 | 2-Cyclohexylethyl 4-methylbenzenesulfonate | HCID 11426070 | — |
| 生成物 | Methyl 5-(2-cyclohexylethoxy)-2-hydroxybenzoate | HCID 19036723 | 43% |
反応手順
Synthesis was carried out in the same manner as in Example 1, except for replacing methyl 2,4-dihydroxybenzoate with methyl 2,5-dihydroxybenzoate and replacing 2-ethylhexyl bromide with 2-cyclohexylethyl p-toluenesulfonate, to obtain methyl 5-(2-cyclohexylethoxy)-2-hydroxybenzoate represented by the following chemical formula (hereinafter referred to as compound 11) as a pale yellow solid in a yield of 43%. The analytical results are shown below. ##STR32##
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05646184 |
| 出典データセット | uspto-grants-1997_07 |
| ORD ID | ord-dde65f479bc54da9b6f090eb6743d7ff |
| 出典メモ | uspto-grants-1997_07 |