関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Hippuric Acid | HCID 464 | — |
| 反応物 | Acetic Anhydride | HCID 7918 | — |
| 生成物 | Azlactone | HCID 65073 | — |
反応手順
23.3 gm of hippuric acid and 93.05 gm of acetic anhydride were charged into a 500 ml eggplant-type flask, and heated on an oil bath at a temperature of 90° C. for 10 minutes. Immediately after the mixture became transparent, it was quenched and kept at 1°-2° C. in ice-water.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05646291 |
|---|
| 出典データセット | uspto-grants-1997_07 |
|---|
| ORD ID | ord-6f79e5d18511406ebb7adf053fcb96c5 |
|---|
| 出典メモ | uspto-grants-1997_07 |
|---|
