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Potassium Carbonate → 7-(3,4,5-Triphenyl-2-oxo-2,3-dihydroimidazol-1-yl)heptanonitrile
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | Heptanenitrile, 7-bromo- | HCID 88737 | — |
| 反応物 | 1,4,5-Triphenyl-1,3-dihydro-2H-imidazol-2-one | HCID 628544 | — |
| 溶媒 | Methyl Ethyl Ketone | HCID 6569 | — |
| 生成物 | 7-(3,4,5-Triphenyl-2-oxo-2,3-dihydroimidazol-1-yl)heptanonitrile | HCID 22916372 | — |
反応手順
1,4,5-Triphenylimidazol-2-one was treated with 7-bromo-heptanonitrile and potassium carbonate in butanone to give after chromatographic work-up 7-(3,4,5-triphenyl-2-oxo-2,3-dihydroimidazol-1-yl)heptanonitrile, m.p. 100°-101° C., Found: C, 79.7; H, 6.6; N, 9.8%; C28H27N3O requires: C, 79.9; H, 6.4; N, 10.0%; and
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05648373 |
| 出典データセット | uspto-grants-1997_07 |
| ORD ID | ord-651a0eb968ab4abe943762bc02b8d73d |
| 出典メモ | uspto-grants-1997_07 |