4-Propyl-4-phenyl-4-silacyclohexanone → HCID 178418359、化合物

反応式

C([Si:4]1([C:11]2[CH:16]=[CH:15]C=CC=2)[CH2:9][CH2:8][C:7](=O)[CH2:6][CH2:5]1)CC.Br[C:18]1[CH:23]=[C:22](F)[C:21]([C:25]([Cl:28])=[CH:26][Cl:27])=[C:20](F)[CH:19]=1>>[CH2:11]([Si@H:4]1[CH2:5][CH2:6][C@H:7]([C:18]2[CH:23]=[CH:22][C:21]([C:18]3[CH:23]=[CH:22][C:21]([C:25]([Cl:28])=[CH:26][Cl:27])=[CH:20][CH:19]=3)=[CH:20][CH:19]=2)[CH2:8][CH2:9]1)[CH2:16][CH3:15]

参加物

反応物 2

HCID 118313174-Propyl-4-phenyl-4-silacyclohexanone

HCID 539779734-Bromo-2,6-difluoro-1-(1,2-dichlorovinyl)benzene

生成物 1

HCID 178418359HCID 178418359、化合物

実験手順

The general procedure of Example 35 was repeated using 4-propyl-4-phenyl-4-silacyclohexanone instead of 4-pentyl-4-phenyl-4-silacyclohexanone, and 4-bromo-2,6-difluoro-1-(1,2-dichlorovinyl)benzene instead of 4-bromo-2,6-difluoro-1-(2,2-difluorovinyloxy)benzene, thereby obtaining the intended compound.

後処理

customobtaining the intended compound

出典と根拠

ORDレコード: ord-db385b2cb2e1457ba6d59349cf5dd028
出典データセット: uspto-grants-1998_03
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05730901

反応ノート

読み込み中…

参加物