化工社化工社 化学情報印刷レポート · 研究参考用
1-Methylimidazole → HCID 178443590、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Methylimidazole | HCID 1390 | — |
| 反応物 | 1-Bromooctane | HCID 8140 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | HCID 178443590 | HCID 178443590 | 90.8% |
反応手順
1 mole of 1-methylimidazole was dissolved in 400 ml of ethanol and 1.2 moles of n-octyl bromide were added. The mixture was then heated to the boiling point for 5 hours. Thereafter, ethanol and excess n-octyl bromide were removed. The residue was purified in ether. In this manner, 250 g of 1-n-octyl-3-methyl-imidazolium bromide were obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04150967 |
| 出典データセット | uspto-grants-1979_04 |
| ORD ID | ord-5d047517faa743fd9d5633632be4f1d5 |
| 出典メモ | uspto-grants-1979_04 |