関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Ethanol | HCID 702 | — |
| 反応物 | Ethylenediamine | HCID 3301 | — |
| 反応物 | N,N'-Diacetyl-L-cystine | HCID 6995101 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Ethylenediaminium N,N'-diacetyl-L-cystinate | HCID 131718838 | 52.2% |
反応手順
To N,N'-Diacetyl-L-cystine (30.9 mmol, 10 g) dissolved in 20 mL of water was added ethylenediamine (61.8 mmol, 3.73 g) and ethanol (30 mL). The solution was concentrated to a thick paste which was redissolved in 80 mL of ethanol. Crystallisation occurred after 2 hours stirring at 10° C. Filtration and drying gave 6.2 g (45%) of the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05650538 |
|---|
| 出典データセット | uspto-grants-1997_07 |
|---|
| ORD ID | ord-e3d5b529b7f841db9859bda0daa1c344 |
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| 出典メモ | uspto-grants-1997_07 |
|---|
