反応式
[NH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][NH2:7].S([O-])([O-])(=O)=O.CS[C:15]([NH2:27])=[NH+:16][CH2:17][CH2:18][S:19][CH2:20][C:21]1[N:22]=[CH:23][NH:24][C:25]=1[CH3:26].CS[C:30]([NH2:42])=[NH+:31][CH2:32][CH2:33][S:34][CH2:35][C:36]1[N:37]=[CH:38][NH:39][C:40]=1[CH3:41]>>[CH3:41][C:40]1[NH:39][CH:38]=[N:37][C:36]=1[CH2:35][S:34][CH2:33][CH2:32][N:31]=[C:30]([NH2:42])[NH:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][NH:7][C:15]([NH2:27])=[N:16][CH2:17][CH2:18][S:19][CH2:20][C:21]1[N:22]=[CH:23][NH:24][C:25]=1[CH3:26]参加物
3
実験手順
The reaction of 1,5-diaminopentane (0.43 g) with S-methyl-N-[2-((5-methyl-4-imidazolyl)methylthio)ethyl]thiouronium sulphate (2.52 g) by the method described in Example 5 afforded the title compound which was isolated as the dipicrate (1.8 g) m.p. 115°-120°.
出典と根拠
- ORDレコード
- ord-142a4a7c20964376a3661ce3b8f8c531
- 出典データセット
- uspto-grants-1979_04
- 特許番号
- US04151289
関連ノート
読み込み中…