HCID 21556903、化合物 → 5-Nitro-2-hexanone
反応式
[N+]([CH2:4][C:5](C)([OH:13])[CH2:6][CH2:7][CH:8]([N+:10]([O-:12])=[O:11])[CH3:9])([O-])=O>C1C=CC=CC=1>[N+:10]([CH:8]([CH3:9])[CH2:7][CH2:6][C:5](=[O:13])[CH3:4])([O-:12])=[O:11]参加物
3
実験手順
To a solution of 0.91 gram of 1,5-dinitro-2-methyl-2-hexanol in 25 milliliters of benzene there was added 4.2 grams of alumina. The mixture was stirred for 24 hours, and the alumina was removed by filtration. After evaporation of the filtrate there was obtained 0.29 gram of 5-nitro-2-hexanone which was identified by infrared and proton magnetic resonance.
後処理
- customthe alumina was removed by filtration
- customAfter evaporation of the filtrate there
出典と根拠
- ORDレコード
- ord-a1ec2d07712f4be1ad68c7b6ff1c2dd1
- 出典データセット
- uspto-grants-1976_03
- 特許番号
- US03941846
反応ノート
読み込み中…