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6H-Dibenzo(b,d)pyran-1-ol, 7,8,9,10-tetrahydro-3-(1,2-dimethylheptyl)-6,6,10-trimethyl- → 3-(3-methyl-2-octyl)-1-[4-(pyrrolidino)-butyryloxy]-7,8,9,10-tetrahydro-6,6,10-trimethyl-6H-dibenzo[b,d] pyran hydrochloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 6H-Dibenzo(b,d)pyran-1-ol, 7,8,9,10-tetrahydro-3-(1,2-dimethylheptyl)-6,6,10-trimethyl- | HCID 3045010 | — |
| 反応物 | 4-(Pyrrolidin-1-yl)butanoic acid hydrochloride | HCID 14855682 | — |
| 生成物 | 3-(3-methyl-2-octyl)-1-[4-(pyrrolidino)-butyryloxy]-7,8,9,10-tetrahydro-6,6,10-trimethyl-6H-dibenzo[b,d] pyran hydrochloride | HCID 68135694 | — |
反応手順
1-Hydroxy-3-(3-methyl-2-octyl)-7,8,9,10-tetrahydro-6,6,10-trimethyl-6H-dibenzo[ b,d] pyran from Example 32 is reacted with γ-pyrrolidinobutyric acid hydrochloride following the procedure of Example 9 to produce 3-(3-methyl-2-octyl)-1-[4-(pyrrolidino)-butyryloxy]-7,8,9,10-tetrahydro-6,6,10-trimethyl-6H-dibenzo[ b,d] pyran hydrochloride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US03941782 |
| 出典データセット | uspto-grants-1976_03 |
| ORD ID | ord-9191a0948b794d8b99645a2735df241f |
| 出典メモ | uspto-grants-1976_03 |