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Dimethylcarbamoyl Chloride → alpha-Diethylcarbamylthio-2'-chloro-4-biphenylylacetic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dimethylcarbamoyl Chloride | HCID 6598 | — |
| 反応物 | Diethylcarbamoyl chloride | HCID 6916 | — |
| 反応物 | Carbamic chloride | HCID 68048 | — |
| 反応物 | N-ethylcarbamoyl chloride | HCID 12321963 | — |
| 反応物 | alpha-Carbamylthio2'-chloro-4-biphenylylacetic acid | HCID 21556048 | — |
| 反応物 | alpha-Dimethylcarbamylthio-2'-chloro-4-biphenylylacetic acid | HCID 21556323 | — |
| 反応物 | alpha-Ethylcarbamylthio-2'-chloro-4-biphenylylacetic acid | HCID 54353825 | — |
| 生成物 | alpha-Diethylcarbamylthio-2'-chloro-4-biphenylylacetic acid | HCID 21556371 | — |
反応手順
When diethylcarbamylchloride is replaced in the above procedure by carbamyl chloride (prepared in situ from potassium cyanate and anhydrous hydrogen chloride in anhydrous chloroform), ethylcarbamyl chloride or dimethylcarbamyl chloride, then the products prepared are α-carbamylthio2'-chloro-4-biphenylylacetic acid, α-ethylcarbamylthio-2'-chloro-4-biphenylylacetic acid or α-dimethylcarbamylthio-2'-chloro-4-biphenylylacetic acid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US03941821 |
| 出典データセット | uspto-grants-1976_03 |
| ORD ID | ord-92812363b4e14ecfb4da9e08a1558a01 |
| 出典メモ | uspto-grants-1976_03 |