化工社化工社 化学情報印刷レポート · 研究参考用
1-Butanol → 2-Hydroxydecyl-butyl ether
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Butanol | HCID 263 | — |
| 反応物 | Ethylene Oxide | HCID 6354 | — |
| 反応物 | 1,2-Epoxydecane | HCID 16993 | — |
| 反応物 | Sodium | HCID 5360545 | — |
| 触媒 | Sodium Methoxide | HCID 10942334 | — |
| 生成物 | 2-Hydroxydecyl-butyl ether | HCID 10466415 | — |
反応手順
As described in Example 1, 1 mol of 1,2-epoxydecane was caused to react with 5 times the molar quantity of n-butanol and 0.04 gm-atom of sodium. After distillation of the excess alcohol, the reaction with 10 mols of ethylene oxide was conducted in an autoclave under the conditions described in Example 1, except for the addition of the sodium methylate catalyst. The product thus obtained had a cloud point of 64°C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US03943178 |
| 出典データセット | uspto-grants-1976_03 |
| ORD ID | ord-5d32d71825f34bd8a73662fac1561a93 |
| 出典メモ | uspto-grants-1976_03 |