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Phenylphosphonic Acid → Adipic Acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Phenylphosphonic Acid | HCID 15295 | — |
| 反応物 | Hexamethylenediamine | HCID 16402 | — |
| 反応物 | 6-Azaniumylhexylazanium;hexanedioate | HCID 27358 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Adipic Acid | HCID 196 | — |
反応手順
A mixture of 100 parts of hexamethylene diammonium adipate, 0.65 part of phenylphosphonic acid, 0.48 part of hexamethylenediamine, 0.65 part of N:N'-bis(3-aminopropyl)piperazine, 0.46 part of adipic acid and 65.0 parts of water is polymerised using the conditions described in Example 1. The resulting polymer is then converted into fibres by known methods. The dye uptake of these fibres from dyebaths containing Solway Blue BN at pH's of 4.0, 7.0 and 9.0 are 8.4%, 4.7% and 1.5% respectively, compared with 4.2%, 0.6% and 0.1% for fibres prepared as described in this Example except that the phenylphosphonic acid and hexamethylenediamine were omitted from the mixture.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US03944518 |
| 出典データセット | uspto-grants-1976_03 |
| ORD ID | ord-e71604194418479ea58f3e9332e592d0 |
| 出典メモ | uspto-grants-1976_03 |