化工社化工社 化学情報印刷レポート · 研究参考用
Citronellal → Rac.-1-benzyloxy-2,6,10-trimethyl-9-undecen-4-ol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Citronellal | HCID 7794 | — |
| 反応物 | ((3-Bromo-2-methylpropoxy)methyl)benzene | HCID 2735492 | — |
| 生成物 | Rac.-1-benzyloxy-2,6,10-trimethyl-9-undecen-4-ol | HCID 20349060 | — |
反応手順
This compound was prepared starting from the rac. 3-benzyloxy-2-methyl-1-propyl bromide and racemic citronellal using the procedure described in Example 4. Rac.-1-benzyloxy-2,6,10-trimethyl-9-undecen-4-ol was obtained as a colorless oil, b.p. 145°-150° C. (bath temperature) (0.01 mm Hg.).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04151205 |
| 出典データセット | uspto-grants-1979_04 |
| ORD ID | ord-2179a3dab9e34f2aa76a3a51ff615773 |
| 出典メモ | uspto-grants-1979_04 |