化工社化工社 化学情報印刷レポート · 研究参考用
Isobutylene → Rac.-methyl 3-tert. butoxy-2-methylpropionate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Isobutylene | HCID 8255 | — |
| 反応物 | Methyl 3-hydroxy-2-methylpropanoate | HCID 521128 | — |
| 生成物 | Rac.-methyl 3-tert. butoxy-2-methylpropionate | HCID 12923318 | 43.5% |
反応手順
Treatment of rac. methyl-3-hydroxy-2-methylpropionate with isobutylene using the procedure described in Example 1 gave rac.-methyl 3-tert. butoxy-2-methylpropionate in 43.5% yield as a colorless liquid. b.p. 75°-85° C. (bath temperature) (11 mm Hg.).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04151205 |
| 出典データセット | uspto-grants-1979_04 |
| ORD ID | ord-25b62f0aefa74641aa740ab860526827 |
| 出典メモ | uspto-grants-1979_04 |