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Potassium Carbonate → N-(1,3-dioxolan-2-ylmethyl)-2-ethyl-6-methylaniline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | 2-Ethyl-6-methylaniline | HCID 32485 | — |
| 反応物 | 2-(Chloromethyl)-1,3-dioxolane | HCID 75727 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | N-(1,3-dioxolan-2-ylmethyl)-2-ethyl-6-methylaniline | HCID 21435679 | — |
反応手順
2-Ethyl-6-methylaniline (70 grams), 2-chloromethyl-1,3-dioxolane (30 grams), potassium carbonate (38 grams) and dimethylformamide (50 ml) were charged into a glass reaction vessel equipped with a mechanical stirrer, thermometer and reflux condenser. The reaction mixture was heated at reflux for a period of about 24 hours. After this time the mixture was filtered and distilled to yield the desired product N-(1,3-dioxolan-2-ylmethyl)-2-ethyl-6-methylaniline.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US03946044 |
| 出典データセット | uspto-grants-1976_03 |
| ORD ID | ord-f766387d9da6484f9e3a7c4a6a0b5b59 |
| 出典メモ | uspto-grants-1976_03 |