関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Tyramine | HCID 5610 | — |
| 反応物 | Triethylammonium hydrogen carbonate | HCID 11768884 | — |
| 反応物 | n-Hydroxysuccinimide biotin | HCID 86743017 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | Biotin tyramine | HCID 86746652 | — |
反応手順
a solution of biotin-N-hydroxysuccinimide, 170 mg (0.5 mMoles), and tyramine (recrystallized from water), 68.5 mg (0.5 mMoles), in 25 ml dimethylformamide was treated with 10 ml of 1M triethylammonium bicarbonate, pH 7.5, and then heated at 50° C. for 3 hours.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05731158 |
|---|
| 出典データセット | uspto-grants-1998_03 |
|---|
| ORD ID | ord-989c68d91dfc4d74a9b62cfdff0165f9 |
|---|
| 出典メモ | uspto-grants-1998_03 |
|---|
