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Chlorotriethylsilane → 3-Triethylsilyl-2-oxazolidinone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Chlorotriethylsilane | HCID 13819 | — |
| 反応物 | 2-Oxazolidinone | HCID 73949 | — |
| 生成物 | 3-Triethylsilyl-2-oxazolidinone | HCID 21454776 | — |
反応手順
Following the previous example, but replacing the trimethylchlorosilane with triethylchlorosilane (63.3 g; 0.42 mol) and operating under similar conditions, the result is the compound of the above heading; a colorless fluid liquid, obtained with a similar yield. 2-oxazolidinone, calculated: 42.82%; found; 42.70%. Distills at 100°C between 2 and 4 mm.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US03947465 |
| 出典データセット | uspto-grants-1976_03 |
| ORD ID | ord-158e83453e7449beb90a25edd87432d5 |
| 出典メモ | uspto-grants-1976_03 |