Phenyl formate → HCID 21552229、化合物

HRID 268462

反応式

HRID 268462 の反応式
[CH3:1][C:2]([NH2:15])([CH2:13][CH3:14])[CH2:3][C:4]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[NH:6][CH:5]=1.[CH:16](OC1C=CC=CC=1)=[O:17]>>[CH3:1][C:2]([NH:15][CH:16]=[O:17])([CH2:13][CH3:14])[CH2:3][C:4]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[NH:6][CH:5]=1

参加物

3

反応物 2

HCID 74626Phenyl formateHCID 21552235HCID 21552235、化合物

生成物 1

HCID 21552229HCID 21552229、化合物

実験手順

The 3-(2'-methyl-2'-aminobutyl)-indole obtained as reduction product in accordance with Example 1 or 3 was reacted with phenyl formate to yield 3-(2'-methyl-2'-formylaminobutyl)-indole; melting point 121.5°-124.5°C. (from ether). Reduction thereof with LiAlH4 yielded 3-(2'-methyl-2'-methylaminobutyl)-indole having a melting point of 100°-103°C. (from cyclohexane).

出典と根拠

ORDレコード
ord-8f956a4918304bc2a1e7c1de3a525c8b
出典データセット
uspto-grants-1976_03
特許番号
US03947584

関連ノート

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