Tetrafluoro-m-phenylenediamine dihydrochloride → 4-(4-Amino-2-methylphenylamino)butan-2-ol dihydrochloride
反応式
[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([NH:10][CH2:11][CH2:12][CH:13]([OH:15])[CH3:14])=[C:6]([CH3:16])[CH:5]=1)([O-])=O.C1(N)C(F)=C(F)C(F)=C(N)C=1F.[ClH:29].Cl>[Zn].[Cl-].[NH4+].O.C(O)C>[ClH:29].[ClH:29].[NH2:1][C:4]1[CH:9]=[CH:8][C:7]([NH:10][CH2:11][CH2:12][CH:13]([OH:15])[CH3:14])=[C:6]([CH3:16])[CH:5]=1参加物
4
実験手順
The 4-(4-nitro-2-methylphenylamino)butan-2-ol (27) obtained above was reduced with a boiling zinc/ammonium chloride/water/ethanol mixture. The corresponding amine was isolated in dihydrochloride form.
出典と根拠
- ORDレコード
- ord-4c11cee63ef64e76bcba09e523cf8b54
- 出典データセット
- uspto-grants-2008_11
- 特許番号
- US07445645B2
反応ノート
読み込み中…