化工社化工社 化学情報印刷レポート · 研究参考用
Pentachlorophenol → 2,4,6-Trichlorophenol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Pentachlorophenol | HCID 992 | — |
| 反応物 | Phenol | HCID 996 | — |
| 生成物 | 2,4,6-Trichlorophenol | HCID 6914 | — |
反応手順
About 143 g of phenol (an amount that should lead to an equivalent amount of pentachlorophenol product, by moles, obtained when about 300 g of 2,4,6-trichlorophenol is used) were added to a reactor at 60° C. with 0.75 g of AlCl3 (about 0.25 wt. % based on trichlorophenol). The same stirring rate (100-120 RPM) and chlorine flow rate (1.5 mol/hr) as experiments that started with trichlorophenol were used.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07446235B2 |
| 出典データセット | uspto-grants-2008_11 |
| ORD ID | ord-eb9c84498fdf4d9ea97bd148c5c5a5ee |
| 出典メモ | uspto-grants-2008_11 |