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HRID 269440作成日:2026年10月27日

Pentachlorophenol → 2,4,6-Trichlorophenol

https://huagongshe.com/reaction/269440

反応式

関与物質

役割名称HCID仕込み量
反応物PentachlorophenolHCID 992—
反応物PhenolHCID 996—
生成物2,4,6-TrichlorophenolHCID 6914—

反応手順

About 143 g of phenol (an amount that should lead to an equivalent amount of pentachlorophenol product, by moles, obtained when about 300 g of 2,4,6-trichlorophenol is used) were added to a reactor at 60° C. with 0.75 g of AlCl3 (about 0.25 wt. % based on trichlorophenol). The same stirring rate (100-120 RPM) and chlorine flow rate (1.5 mol/hr) as experiments that started with trichlorophenol were used.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07446235B2
出典データセットuspto-grants-2008_11
ORD IDord-eb9c84498fdf4d9ea97bd148c5c5a5ee
出典メモuspto-grants-2008_11