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Phenethylamine → N-[[2-[2-(4-Morpholinyl)ethoxy]phenyl]methylene]benzeneethanamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Phenethylamine | HCID 1001 | — |
| 反応物 | 2-(2-Morpholinoethoxy)benzaldehyde | HCID 976593 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | N-[[2-[2-(4-Morpholinyl)ethoxy]phenyl]methylene]benzeneethanamine | HCID 21322775 | 85.6% |
反応手順
2-[2-(4-Morpholinyl)ethoxy]benzaldehyde (55.9 g) is reacted with 29 g of phenethylamine in 240 ml of toluene following the procedure described in Example 1A to yield 68.8 g of product as an oil, boiling point 204°-210° C. at 0.1-0.2 mm of Hg.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04151354 |
| 出典データセット | uspto-grants-1979_04 |
| ORD ID | ord-4ac30af58cde4ba28f2ed7a5aea79b00 |
| 出典メモ | uspto-grants-1979_04 |