化工社化工社 化学情報印刷レポート · 研究参考用
2-Amino-4-chlorophenol → 2-Acetylamino-4-chlorophenol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Amino-4-chlorophenol | HCID 7265 | — |
| 反応物 | Acetic Anhydride | HCID 7918 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | 2-Acetylamino-4-chlorophenol | HCID 95258 | 80.8% |
反応手順
To a suspension of 2-amino-4-chlorophenol (1.43 g, 10.0 mmol) in methanol was added acetic anhydride (0.945 mL, 10.0 mmol) and the reaction mixture was stirred at room temperature for 2 h. The volatiles were removed in vacuo to give the subtitled compound (1.5 g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07449475B2 |
| 出典データセット | uspto-grants-2008_11 |
| ORD ID | ord-40c22dff81724e1d9b69e1626f222a07 |
| 出典メモ | uspto-grants-2008_11 |