化工社化工社 化学情報印刷レポート · 研究参考用
Methyl Salicylate → N-Methylsalicylamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl Salicylate | HCID 4133 | — |
| 反応物 | Methylamine | HCID 6329 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | N-Methylsalicylamide | HCID 74624 | 90.6% |
反応手順
A solution of methyl salicylate (5.16 mL, 40 mmol) in methanol (10 mL) was added dropwise to aqueous 40% methylamine (18.1 mL, 210 mmol) at 0° C. After addition was complete the reaction mixture was kept on stirring at room temperature overnight. The volatiles were removed in vacuo to give the subtitled compound (5.48 g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07449475B2 |
| 出典データセット | uspto-grants-2008_11 |
| ORD ID | ord-6df448f464b946efb1c50dd83b17c1f4 |
| 出典メモ | uspto-grants-2008_11 |