化工社化工社 化学情報印刷レポート · 研究参考用
N-(2-Methoxyethyl)ethylamine → [3-[3-(4-Bromo-phenyl)-benzo[d]isothiazol-6-yloxy]-propyl]-ethyl-(2-methoxy-ethyl)-amine hydrobromide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-(2-Methoxyethyl)ethylamine | HCID 546877 | — |
| 反応物 | HCID 22314069 | HCID 22314069 | — |
| 生成物 | [3-[3-(4-Bromo-phenyl)-benzo[d]isothiazol-6-yloxy]-propyl]-ethyl-(2-methoxy-ethyl)-amine hydrobromide | HCID 22313889 | — |
反応手順
In analogy to example 3.1, 3-(4-Bromo-phenyl)-6-(3-bromo-propoxy)-benzo[d]isothiazole and N-(2-methoxyethyl)ethylamine were converted to yield (without extraction) [3-[3-(4-Bromo-phenyl)-benzo[d]isothiazol-6-yloxy]-propyl]-ethyl-(2-methoxy-ethyl)-amine hydrobromide as colorless oil, MS: 449(MH+, 1Br).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07449483B2 |
| 出典データセット | uspto-grants-2008_11 |
| ORD ID | ord-3531673cb1b746a4b5ef9085c445dbd7 |
| 出典メモ | uspto-grants-2008_11 |