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3-Methoxybenzenethiol → 2-Methyl-3-(4-trifluoromethyl-phenyl)-benzo[b]thiophen-6-ol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Methoxybenzenethiol | HCID 84989 | — |
| 反応物 | 2-Bromo-1-(4-(trifluoromethyl)phenyl)propan-1-one | HCID 10423819 | — |
| 生成物 | 2-Methyl-3-(4-trifluoromethyl-phenyl)-benzo[b]thiophen-6-ol | HCID 17932879 | — |
反応手順
In analogy to examples 26.1-26.3, 3-Mercaptoanisole and 2-Bromo-1-(4-trifluoromethyl-phenyl)-propan-1-one were converted to yield 2-Methyl-3-(4-trifluoromethyl-phenyl)-benzo[b]thiophen-6-ol as colorless amorphous solid, MS: 308 (M).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07449483B2 |
| 出典データセット | uspto-grants-2008_11 |
| ORD ID | ord-1f4f2856f53b428eaa185762d9c4eb48 |
| 出典メモ | uspto-grants-2008_11 |