2-(Ethylamino)ethanol → 2-[Ethyl-(1-methyl-prop-2-ynyl)-amino]-ethanol

反応式

[CH3:1][CH:2](O)[C:3]#[CH:4].[CH2:6]([NH:8][CH2:9][CH2:10][OH:11])[CH3:7]>>[CH2:6]([N:8]([CH:2]([CH3:1])[C:3]#[CH:4])[CH2:9][CH2:10][OH:11])[CH3:7]

参加物

反応物 2

HCID 80722-(Ethylamino)ethanol

HCID 162393-Butyn-2-ol

生成物 1

HCID 223140542-[Ethyl-(1-methyl-prop-2-ynyl)-amino]-ethanol

実験手順

In analogy to example 37.5 and 37.6, 3-Butyn-2-ol and 2-Ethylaminoethanol were converted to yield 2-[Ethyl-(1-methyl-prop-2-ynyl)-amino]-ethanol as colorless oil, MS: 141 (M).

出典と根拠

ORDレコード: ord-68d1c453b3c64b0bbc86532d375a7203
出典データセット: uspto-grants-2008_11
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US07449483B2

反応ノート

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