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1,1-Bis(methylthio)-2-nitroethylene → 1-Nitro-2-methylthio-2-[4-(4-imidazolyl)butylamino]ethylene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,1-Bis(methylthio)-2-nitroethylene | HCID 83623 | — |
| 反応物 | HCID 178510959 | HCID 178510959 | — |
| 溶媒 | Acetonitrile | HCID 6342 | — |
| 生成物 | 1-Nitro-2-methylthio-2-[4-(4-imidazolyl)butylamino]ethylene | HCID 178503821 | — |
反応手順
A solution of 4-(4-aminobutyl)imidazole (from the dihydrobromide (3.6 g)) and 1-nitro-2,2-bis-methylthioethylene (2.0 g) in acetonitrile (50 ml) was set aside at room temperature for 3 days. The product was chromatographed on a column of silica gel to give 1-nitro-2-methylthio-2-[4-(4-imidazolyl)butylamino]ethylene.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04220652 |
| 出典データセット | uspto-grants-1980_09 |
| ORD ID | ord-b946b297dc4c49f18af7ef3af86d6d42 |
| 出典メモ | uspto-grants-1980_09 |