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1,1-Bis(methylthio)-2-nitroethylene → 1-Nitro-2-methylthio-2-[3-(2-oxazolylthio)propylamino]ethylene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,1-Bis(methylthio)-2-nitroethylene | HCID 83623 | — |
| 反応物 | 2-(3-Aminopropyl)thiooxazole | HCID 20550119 | — |
| 生成物 | 1-Nitro-2-methylthio-2-[3-(2-oxazolylthio)propylamino]ethylene | HCID 70541392 | 63% |
反応手順
By the procedure of Example 8(i), 2-(3-aminopropylthio)oxazole (2.1 g) is reacted with 1-nitro-2,2-bis-methylthioethylene (2.0 g) to give 1-nitro-2-methylthio-2-[3-(2-oxazolylthio)propylamino]ethylene (2.1 g) which, on reaction with methylamine by the procedure of Example 8(ii) gives the title product (1.8 g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04220652 |
| 出典データセット | uspto-grants-1980_09 |
| ORD ID | ord-db6bb7fbc6ad4f9b830b4d94e9cb2908 |
| 出典メモ | uspto-grants-1980_09 |