Propanedinitrile, 2-[(methylamino)(methylthio)methylene]- → 1,1-Dicyano-2-methylamino-2-[2-(3-isothiazolylmethylthio)-ethylamino]ethylene

反応式

[NH2:1][CH2:2][CH2:3][S:4][CH2:5][C:6]1[CH:10]=[CH:9][S:8][N:7]=1.[C:11]([C:13]([C:19]#[N:20])=[C:14](SC)[NH:15][CH3:16])#[N:12]>>[C:11]([C:13]([C:19]#[N:20])=[C:14]([NH:15][CH3:16])[NH:1][CH2:2][CH2:3][S:4][CH2:5][C:6]1[CH:10]=[CH:9][S:8][N:7]=1)#[N:12]

参加物

反応物 2

HCID 3640288Propanedinitrile, 2-[(methylamino)(methylthio)methylene]-

HCID 129515372-{[(1,2-Thiazol-3-yl)methyl]sulfanyl}ethan-1-amine

生成物 1

HCID 205502261,1-Dicyano-2-methylamino-2-[2-(3-isothiazolylmethylthio)-ethylamino]ethylene

実験手順

By the procedure of Example 1(ii), reacting 3-[(2-aminoethyl)thiomethyl]isothiazole with 1,1-dicyano-2-methylthio-2-methylaminoethylene gives the title compound.

出典と根拠

ORDレコード: ord-993125988fcb4920b6dab00407f91267
出典データセット: uspto-grants-1980_09
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04220652

反応ノート

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