化工社化工社 化学情報印刷レポート · 研究参考用
Aniline → 2-[(N-phenylcarbamoyl)methyl]prop-2-enoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Aniline | HCID 6115 | — |
| 反応物 | Itaconic Anhydride | HCID 75110 | — |
| 溶媒 | Methyl Chloride | HCID 6327 | — |
| 生成物 | 2-[(N-phenylcarbamoyl)methyl]prop-2-enoic acid | HCID 21935560 | — |
反応手順
A solution of 2-methylenesuccinic anhydride (500 mg, 4.46 mmol) and aniline (0.4 mL, 4.46 mmol) in CH3Cl were shaken overnight. A precipitate formed, which was filtered off, washed with hexanes, and dried under vacuum to afford 2-[(N-phenylcarbamoyl)methyl]prop-2-enoic acid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07452889B2 |
| 出典データセット | uspto-grants-2008_11 |
| ORD ID | ord-682c33e9511d4681b3e6095fa4659f39 |
| 出典メモ | uspto-grants-2008_11 |