反応式
[N:1]([C:4]1[C:5]([NH:11]C(=O)C(C)(C)C)=[N:6][CH:7]=[C:8]([F:10])[CH:9]=1)=[N+:2]=[N-:3].[ClH:18]>>[N:1]([C:4]1[C:5]([NH2:11])=[N:6][CH:7]=[C:8]([F:10])[CH:9]=1)=[N+:2]=[N-:3].[ClH:18]参加物
4
実験手順
N-(3-Azido-5-fluoropyridin-2-yl)-2,2-dimethylpropanamide (275 mg, 1.16 mmol) in 3 N HCl (5 mL) was heated to 100° C. After 2 h, the volatiles were removed in vacuo, to give the title compound as its HCl salt (180 mg). MS 154.2 (M+1).
後処理
- customthe volatiles were removed in vacuo
出典と根拠
- ORDレコード
- ord-321efd9e941f4a5a9155c968db9dec32
- 出典データセット
- uspto-grants-2008_11
- 特許番号
- US07452903B2
関連ノート
読み込み中…