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Phosgene → 2,6-Dimethylpiperidine-1-carbonyl chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Phosgene | HCID 6371 | — |
| 反応物 | Nanofin | HCID 68843 | — |
| 溶媒 | Benzene | HCID 241 | — |
| 生成物 | 2,6-Dimethylpiperidine-1-carbonyl chloride | HCID 19070661 | — |
反応手順
To a solution of 50 g of 2,6-dimethylpiperidine in 300 ml of benzene is added 60 g of phosgene and the mixture is refluxed for 3 hours. The solid which had separated was filtered and the filtrate was concentrated and distilled under vacuum to obtain 2,6-dimethylpiperidinoyl chloride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04220658 |
| 出典データセット | uspto-grants-1980_09 |
| ORD ID | ord-d11774a1636640a29040ec7cd02bfe95 |
| 出典メモ | uspto-grants-1980_09 |