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HRID 272390作成日：2026年10月27日

4-Fluoro-N-(2,2,4,6,7-pentamethyl-3-(4-methylphenyl)-2,3-dihydro-1-benzofuran-5-yl]benzamide → N-(4-Fluorobenzyl)-2,2,4,6,7-pentamethyl-3-(4-methylphenyl)-2,3-dihydro-1-benzofuran-5-amine

https://huagongshe.com/reaction/272390

反応式

関与物質

役割名称HCID仕込み量
反応物4-Fluoro-N-(2,2,4,6,7-pentamethyl-3-(4-methylphenyl)-2,3-dihydro-1-benzofuran-5-yl]benzamideHCID 10202094—
溶媒MethanolHCID 887—
生成物N-(4-Fluorobenzyl)-2,2,4,6,7-pentamethyl-3-(4-methylphenyl)-2,3-dihydro-1-benzofuran-5-amineHCID 993102439%

反応手順

By using 4-fluoro-N-[2,2,4,6,7-pentamethyl-3-(4-methylphenyl)-2,3-dihydro-1-benzofuran-5-yl]benzamide, the title compound was synthesized according to Example 2b. Yield: 39%. Melting point: 92-94° C. (Methanol)

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07456162B2
出典データセットuspto-grants-2008_11
ORD IDord-ada468b769ef428189e01784e43f5d12
出典メモuspto-grants-2008_11