(Pyridin-4-yl)boronic acid → 3-(4-Chloro-2-methoxybenzyl)pyridine
反応式
O1CCCOB1[C:7]1[CH:8]=[N:9][CH:10]=[CH:11][CH:12]=1.Br[CH2:14][C:15]1[CH:20]=[CH:19][C:18]([Cl:21])=[CH:17][C:16]=1[O:22][CH3:23].N1C=CC(B(O)O)=CC=1>>[Cl:21][C:18]1[CH:19]=[CH:20][C:15]([CH2:14][C:7]2[CH:8]=[N:9][CH:10]=[CH:11][CH:12]=2)=[C:16]([O:22][CH3:23])[CH:17]=1参加物
4
実験手順
The title compound was prepared by substituting 1-bromomethyl-4-chloro-2-methoxy-benzene and 3-[1,3,2]dioxaborinan-2-yl-pyridine for 1-bromomethyl-4-chloro-2-methoxy-benzene and 4-pyridyl boronic acid, respectively, in Example 700A. MS (ESI) m/e 234 (M+H)+.
出典と根拠
- ORDレコード
- ord-8d235e009903405580d4e96f80d40714
- 出典データセット
- uspto-grants-2008_11
- 特許番号
- US07456169B2
反応ノート
読み込み中…