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Acetone → 9-Hydroxynonan-2-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetone | HCID 180 | — |
| 反応物 | p-Toluenesulfonic acid monohydrate | HCID 521998 | — |
| 生成物 | 9-Hydroxynonan-2-one | HCID 537408 | — |
反応手順
A solution containing 56.6 g of 8-oxononan-1-ol ethylene ketol (prepared in Example 22 B-5) in 210 ml acetone and 50 mg p-toluenesulfonic acid monohydrate was stirred at room temperature for about 15 to 17 hr. The acetone was removed in vacuo to yield the title compound having the following physical characteristics:
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04220795 |
| 出典データセット | uspto-grants-1980_09 |
| ORD ID | ord-693e33c552514efd8070df5fd9ba4b0a |
| 出典メモ | uspto-grants-1980_09 |