化工社化工社 化学情報印刷レポート · 研究参考用
Sodium Hydroxide → Acifluorfen sodium
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | Acifluorfen | HCID 44073 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | Acifluorfen sodium | HCID 44072 | 105.4% |
反応手順
5-(2-Chloro-4-trifluoromethylphenoxy)-2-nitrobenzoic acid (1.7 g, 0.0047 mole) is dissolved in methanol (25 ml) and sodium hydroxide (4.7 ml of 1 N NaOH in methanol, 0.0047 mole) is added rapidly. The solvent is then removed in vacuo to give 1.9 g of product that decomposes at 217° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04220468 |
| 出典データセット | uspto-grants-1980_09 |
| ORD ID | ord-f721db82d1d0420393e4aedde7b519cb |
| 出典メモ | uspto-grants-1980_09 |