Phenylsulfonyl ketenethioacetal → HCID 178503876、化合物

HRID 27386

反応式

HRID 27386 の反応式
[C:1]1([S:7]([C:10]([C:16]#[N:17])=[C:11]([S:14][CH3:15])SC)(=[O:9])=[O:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:18][C:19]1[N:20]=[CH:21][NH:22][C:23]=1[CH2:24][S:25][CH2:26][CH2:27][NH2:28]>>[C:1]1([S:7]([C:10]([C:16]#[N:17])=[C:11]([S:14][CH3:15])[NH:28][CH2:27][CH2:26][S:25][CH2:24][C:23]2[NH:22][CH:21]=[N:20][C:19]=2[CH3:18])(=[O:8])=[O:9])[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

参加物

3

反応物 2

HCID 194051Phenylsulfonyl ketenethioacetalHCID 178433288HCID 178433288、化合物

生成物 1

HCID 178503876HCID 178503876、化合物

実験手順

Equimolar amounts of 1-benzenesulfonyl-1-cyano-2,2-bis(methylthio)ethylene [prepared according to the procedure described by M. Augustin et al., Z. Chem., 17, 289 (1977)] and 2-[(4-methyl-1H-imidazol-5-yl)methylthio]ethylamine [prepared according to the procedure described in U.S. Pat. No. 3,950,353] are reacted according to the general procedure of Example 6A, and the title product is produced.

後処理

  1. custom3,950,353] are reacted

出典と根拠

ORDレコード
ord-159cb7efc2f84e90b3701ceb6e2e89f7
出典データセット
uspto-grants-1980_09
特許番号
US04221737

関連ノート

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