3,5-Di-tert-butyl-4-hydroxybenzaldehyde → 5-[[3,5-Bis(1,1-dimethylethyl)-4-hydroxyphenyl]methylene]-3-dimethylamino-2-thioxo-4-thiazolidinone

HRID 273887

反応式

HRID 273887 の反応式
[C:1]([C:5]1[CH:6]=[C:7]([CH:10]=[C:11]([C:14]([CH3:17])([CH3:16])[CH3:15])[C:12]=1[OH:13])[CH:8]=O)([CH3:4])([CH3:3])[CH3:2].[CH3:18][N:19]([CH3:27])[N:20]1[C:24](=[O:25])[CH2:23][S:22][C:21]1=[S:26]>>[CH3:4][C:1]([C:5]1[CH:6]=[C:7]([CH:8]=[C:23]2[S:22][C:21](=[S:26])[N:20]([N:19]([CH3:27])[CH3:18])[C:24]2=[O:25])[CH:10]=[C:11]([C:14]([CH3:17])([CH3:16])[CH3:15])[C:12]=1[OH:13])([CH3:2])[CH3:3]

参加物

3

反応物 2

HCID 732193,5-Di-tert-butyl-4-hydroxybenzaldehydeHCID 43419784(5H)-Thiazolone, 3-(dimethylamino)dihydro-2-thioxo-

生成物 1

HCID 544777015-[[3,5-Bis(1,1-dimethylethyl)-4-hydroxyphenyl]methylene]-3-dimethylamino-2-thioxo-4-thiazolidinone収率 65%

実験手順

The title compound was prepared in 65% yield from 3,5-di-tert-butyl-4-hydroxybenzaldehyde and N-dimethylaminorhodanine following the procedure of Example 1.

出典と根拠

ORDレコード
ord-3fc53c58da5541b7be879e3d056e8312
出典データセット
uspto-grants-1995_02
特許番号
US05387690

関連ノート

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