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2-(4-chlorobenzyl)-4,5,6,7-tetrahydro-3H-azepine → 2-[(4-Chlorophenyl)methyl]azepane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-(4-chlorobenzyl)-4,5,6,7-tetrahydro-3H-azepine | HCID 23342815 | — |
| 触媒 | Platinum | HCID 23939 | — |
| 生成物 | 2-[(4-Chlorophenyl)methyl]azepane | HCID 3933809 | — |
反応手順
Hydrogenate the thus-obtained 2-(4-chlorobenzyl)-4,5,6,7-tetrahydro-3H-azepine with platinum/active carbon/ hydrogen. Filter out the catalyst, concentrate the filtrate and distil to obtain 61.9 g (68% of theory) of the title compound with a BP of 93° at 0.1 mm of Hg.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04221788 |
| 出典データセット | uspto-grants-1980_09 |
| ORD ID | ord-a9a8a7247d0e458c9769f6464a652878 |
| 出典メモ | uspto-grants-1980_09 |