Ethyl isobutyrate → Ethyl 6-bromo-2,2-dimethylhexanoate

反応式

[C:1]([O:6][CH2:7][CH3:8])(=[O:5])[CH:2]([CH3:4])[CH3:3].[Br:9][CH2:10][CH2:11][CH2:12][CH2:13]Br>>[Br:9][CH2:10][CH2:11][CH2:12][CH2:13][C:2]([CH3:4])([CH3:3])[C:1]([O:6][CH2:7][CH3:8])=[O:5]

参加物

反応物 2

HCID 7342Ethyl isobutyrate

HCID 80561,4-Dibromobutane

生成物 1

HCID 10444833Ethyl 6-bromo-2,2-dimethylhexanoate

実験手順

Using ethyl isobutyrate and 1,4-dibromobutane, the same reaction as in Reference Example 16 was conducted to produce the title compound. b.p. 62°-64° C./0.4 mmHg

後処理

customthe same reaction as in Reference Example 16

出典と根拠

ORDレコード: ord-361c836d642547cb80dc49089ba624f5
出典データセット: uspto-grants-1995_02
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05389633

反応ノート

読み込み中…