関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 3,4-Diaminopyridine | HCID 5918 | — |
| 反応物 | Pentanoic Acid | HCID 7991 | — |
| 生成物 | HCID 178441556 | HCID 178441556 | 99.6% |
反応手順
A mixture of 3 g of 3,4-diamino-pyridine and 8.28 g of valeric acid was heated to 70° C. for 18 hours and the reaction medium was chromatographed on silica (eluant: ethyl acetatemethanol (8-2)) to obtain 4.8 g of the expected product which was used as is for the following step.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05389634 |
|---|
| 出典データセット | uspto-grants-1995_02 |
|---|
| ORD ID | ord-ad0e57e92b4348ebbe384289d16ea0c2 |
|---|
| 出典メモ | uspto-grants-1995_02 |
|---|
