Methyl 3-benzyloxy-6-phenylpicolinate → Methyl 3-hydroxy-6-phenylpicolinate

HRID 274883ノート

反応式

HRID 274883 の反応式
C([O:8][C:9]1[C:10]([C:21]([O:23][CH3:24])=[O:22])=[N:11][C:12]([C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)=[CH:13][CH:14]=1)C1C=CC=CC=1>[C].[Pd].CO>[OH:8][C:9]1[C:10]([C:21]([O:23][CH3:24])=[O:22])=[N:11][C:12]([C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)=[CH:13][CH:14]=1

参加物

3

反応物 1

HCID 20088897Methyl 3-benzyloxy-6-phenylpicolinate

生成物 1

HCID 15790533Methyl 3-hydroxy-6-phenylpicolinate

試薬・触媒・溶媒 1

HCID 178502579HCID 178502579、化合物触媒

実験手順

1.9 g of methyl 3-benzyloxy-6-phenylpicolinate was reduced with 10% palladium carbon/methanol, and the resultant product was purified by column chromatography to obtain an aimed compound.

後処理

  1. customthe resultant product was purified by column chromatography

出典と根拠

ORDレコード
ord-aad0c75832244ed099f47f2dd9ef22ce
出典データセット
uspto-grants-1995_02
特許番号
US05391537

反応ノート

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