HCID 15239992、化合物 → methyl 6-(N,N-dimethylamino)-3-hydroxypicolinate
反応式
C([O:8][C:9]1[C:10]([C:18]([O:20][CH3:21])=[O:19])=[N:11][C:12]([N:15]([CH3:17])[CH3:16])=[CH:13][CH:14]=1)C1C=CC=CC=1>[C].[Pd].C(OCC)(=O)C>[CH3:17][N:15]([C:12]1[N:11]=[C:10]([C:18]([O:20][CH3:21])=[O:19])[C:9]([OH:8])=[CH:14][CH:13]=1)[CH3:16]参加物
4
実験手順
2.3 g (8 mmol) of methyl 3-benzyloxy-6-(N,N-dimethylamino)picolinate and 0.3 g of 10% palladium carbon were added to 100 ml of ethyl acetate, and was hydrogenated under normal pressure, after the reaction, the reaction product was filtrated and concentrated to obtain a crystal.
後処理
- customafter the reaction
- filtrationthe reaction product was filtrated
- concentrationconcentrated
- customto obtain a crystal
出典と根拠
- ORDレコード
- ord-d4b79056edcf4a36b03943e9afab1acc
- 出典データセット
- uspto-grants-1995_02
- 特許番号
- US05391537
反応ノート
読み込み中…