Sulfuric Acid → alpha,2,6-Trimethylmorpholin-4-ylethanol

HRID 274990

反応式

HRID 274990 の反応式
[OH:1][CH:2]([CH3:13])[CH2:3][N:4]([CH2:9][CH:10]([OH:12])[CH3:11])[CH2:5][CH:6](O)[CH3:7].S(=O)(=O)(O)O>>[OH:1][CH:2]([CH3:13])[CH2:3][N:4]1[CH2:9][CH:10]([CH3:11])[O:12][CH:6]([CH3:7])[CH2:5]1

参加物

3

実験手順

3 g of tris-(2-hydroxypropyl)amine and 1 g of SnO2 doped with sulfuric acid were heated in a manner similar to that described in Example 3 for a period of 1 h at 250° C. There were obtained, in addition to 50 wt % of educt, 30 wt % of N-(2-hydroxypropyl)-2,6-dimethylmorpholine.

後処理

  1. temperaturewere heated in a manner similar to

出典と根拠

ORDレコード
ord-b688cab9275c4fb6885fb2fc7cb74e14
出典データセット
uspto-grants-1995_02
特許番号
US05391734

関連ノート

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