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Ethyl isothiocyanate → HCID 178464567、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl isothiocyanate | HCID 10966 | — |
| 反応物 | CH2N2Pb | HCID 22262466 | — |
| 反応物 | HCID 178465515 | HCID 178465515 | — |
| 反応物 | HCID 178511340 | HCID 178511340 | — |
| 生成物 | HCID 178464567 | HCID 178464567 | — |
反応手順
By the procedure of Example 3(b), reacting N-(3-pyrazolylmethyl)ethylenediamine with ethyl isothiocyanate, then reacting the resulting N-ethyl-N'-[2-(3-pyrazolylmethylamino)ethyl]thiourea with lead cyanamide gives N-cyano-N'-ethyl-N"-[2-(3-pyrazolylmethylamino)ethyl]guanidine. By the same procedure, using propyl isothiocyanate the corresponding N'-propyl compound is prepared. Also, by the same procedure, using 2-dimethylaminoethyl isothiocyanate, the product is N-cyano-N'-(2-dimethylaminoethyl)-N"-[2-(3-pyrazolylmethylamino)ethyl]guanidine.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04221802 |
| 出典データセット | uspto-grants-1980_09 |
| ORD ID | ord-9400006be74740d2b743a43dda1e6d5e |
| 出典メモ | uspto-grants-1980_09 |