関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 2-Methylbenzothiazole | HCID 8446 | — |
| 反応物 | 6-Bromohexanoic acid | HCID 20210 | — |
| 生成物 | 2-Methyl-3-(5-carboxypentyl) benzothiazolium bromide | HCID 22930888 | 212.9% |
反応手順
2-methyl benzothiazole (19.5g, 0.1M) and 6-bromohexanoic acid (15.3g, 0.1M) were mixed and heated at 120° C. for 4 hours under continuous agitation. The resulting solid was broken up, ground with ether and then filtered. The filtrate was washed with more ether (250ml) to yield an off-white powder (57.5g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05393654 |
|---|
| 出典データセット | uspto-grants-1995_02 |
|---|
| ORD ID | ord-e9b9ffc8121942548db3ebc77f1545c8 |
|---|
| 出典メモ | uspto-grants-1995_02 |
|---|
