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HRID 275252作成日:2026年10月27日

1-Phenyl-1,3-propanediol → Hydroxypropiophenone

https://huagongshe.com/reaction/275252

反応式

関与物質

役割名称HCID仕込み量
反応物1-Phenyl-1,3-propanediolHCID 572059—
反応物(1S)-1-phenylpropane-1,3-diolHCID 6950537—
溶媒Isopropanol hexaneHCID 21585144—
生成物HydroxypropiophenoneHCID 569605—

反応手順

Determination of the absolute configuration, optical purity and reaction yield of 1-phenyl-1,3-propanediol or a derivative thereof in the examples was determined by high pressure liquid chromatography (column: Chiral Cell OB, manufactured by Daisel Chemical Co., eluent: hexane/2-propanol (8/2), flow rate: 0.7 ml/min, detection: UV 210 nm). The reaction yield represents the mole percentage of (S)-1-phenyl-1,3-propanediol produced per mole of 1-phenylpropan-3-ol-1-one added as starting material.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05393664
出典データセットuspto-grants-1995_02
ORD IDord-4ea4684372744d47a2f4a72e51f79258
出典メモuspto-grants-1995_02