化工社化工社 化学情報印刷レポート · 研究参考用
N-ethyl-N'-[2-(2-pyrazinylmethylamino)ethyl]thiourea → N-cyano-N'-ethyl-N"-[2-(2-pyrazinylmethylamino)ethyl]-guanidine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-ethyl-N'-[2-(2-pyrazinylmethylamino)ethyl]thiourea | HCID 20567640 | — |
| 反応物 | CH2N2Pb | HCID 22262466 | — |
| 生成物 | N-cyano-N'-ethyl-N"-[2-(2-pyrazinylmethylamino)ethyl]-guanidine | HCID 54105532 | — |
反応手順
Reacting N-(2-pyrazinylmethyl)ethylenediamine with ethyl isothiocyanate by the procedure of Example 3 and chromatographing gives N-ethyl-N'-[2-(2-pyrazinylmethylamino)ethyl]thiourea. Reacting this thiourea with lead cyanamide by the procedure of Example 3 gives N-cyano-N'-ethyl-N"-[2-(2-pyrazinylmethylamino)ethyl]-guanidine.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04221802 |
| 出典データセット | uspto-grants-1980_09 |
| ORD ID | ord-7d07c31946774c9a937670d1f0fe2b07 |
| 出典メモ | uspto-grants-1980_09 |