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HRID 275638作成日:2026年10月26日

Naphthalene → 2-Naphthalenesulfonic acid

https://huagongshe.com/reaction/275638

反応式

関与物質

役割名称HCID仕込み量
反応物NaphthaleneHCID 931—
反応物Sulfuric AcidHCID 1118—
生成物2-Naphthalenesulfonic acidHCID 8420—

反応手順

1,050 g of sulfuric acid was added to 1,280 g of naphthalene, and the reaction was carried out at 160° C. for 2 hours. Unreacted materials were separated and discharged outside the container under a reduced pressure. Then, 857 g of 35% by weight concentration formalin was added and reacted at 105° C. for 5 hours to obtain a condensation product formed by methylene type bonding of β-naphthalene sulfonic acid. After being neutralized with ammonium water, the condensation product was filtrated to yield a filtrate liquid.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US06352651B1
出典データセットuspto-grants-2002_03
ORD IDord-653a541d6544467a92d3c139425373e3
出典メモuspto-grants-2002_03