化工社化工社 化学情報印刷レポート · 研究参考用
Naphthalene → 2-Naphthalenesulfonic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Naphthalene | HCID 931 | — |
| 反応物 | Sulfuric Acid | HCID 1118 | — |
| 生成物 | 2-Naphthalenesulfonic acid | HCID 8420 | — |
反応手順
1,050 g of sulfuric acid was added to 1,280 g of naphthalene, and the reaction was carried out at 160° C. for 2 hours. Unreacted materials were separated and discharged outside the container under a reduced pressure. Then, 857 g of 35% by weight concentration formalin was added and reacted at 105° C. for 5 hours to obtain a condensation product formed by methylene type bonding of β-naphthalene sulfonic acid. After being neutralized with ammonium water, the condensation product was filtrated to yield a filtrate liquid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06352651B1 |
| 出典データセット | uspto-grants-2002_03 |
| ORD ID | ord-653a541d6544467a92d3c139425373e3 |
| 出典メモ | uspto-grants-2002_03 |